Research Article

Rapid and Simultaneous Quantification of Six Aristolochic Acids and Two Lignans in Asari Radix et Rhizoma Using Ultra-Performance Liquid Chromatography-Triple Quadrupole Tandem Mass Spectrometry

Table 3

The representative calibration curve, linear range, LOQs, stability, and repeatability of analytes (n = 3).

CompoundsCalibration curveR 2Linear range (ng/mL)LOQ (ng/mL)Stability (%)Repeatability (%)

AA-IIIy = 20.0228x ^ 0.84670.99815–10005n.d.n.d.
AA-VIIay = 17.0538x ^ 0.94830.99895–100021.185.68
AA-IVay = 73.1555x ^ 0.84500.99855–100021.763.03
AL-Iy = 482.1083x ^ 0.87310.99205–100022.012.72
AA-IIy = 10.4508x ^ 0.86040.99865–10005n.d.n.d.
AA-Iy = 43.3606x ^ 0.98500.99565–100025.456.52
Sesaminy = 7.6321x ^ 0.91390.994250–10000502.274.08
Asarininy = 18.8808x ^ 0.87280.991250–10000502.643.81

n.d., means not detected in samples.