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Journal of Analytical Methods in Chemistry
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Journal of Analytical Methods in Chemistry
/
2014
/
Article
/
Tab 3
/
Research Article
A Stability-Indicating HPLC-DAD Method for Determination of Stiripentol: Development, Validation, Kinetics, Structure Elucidation and Application to Commercial Dosage Form
Table 3
Robustness of the method.
Parameters changed
Variation
Retention time of STP (min)
Peak area*
Bias (%)
Temperature (°C)
23
1.81
303409
−0.31
27
1.80
312560
2.69
Flow rate (mL/min)
0.9
1.83
308654
1.41
1.1
1.77
314565
3.35
pH
3.9
1.79
312468
2.66
4.0
1.78
296265
−2.66
4.2
1.84
304648
0.092
4.3
1.82
289216
−4.98
Peak area of 10
g/mL of STP.