Research Article

A Novel Application of Natural Peat for Solid-Phase Extraction of Pyrimethanil, Flumetralin, and Kresoxim-Methyl in Water Using Gas Chromatography-Mass Spectrometry

Table 1

Influence of different sorbents on pesticide recoveries (RSD%) using dichloromethane as eluting solvent during SPE procedure with GC-MS analysis. Water samples spiked at 2.5  𝜇 g L 1   *( 𝑛 = 7 ).

SorbentRecovery (%) ± RSD (%)*
PyrimethanilFlumetralinKresoxim-methyl

C18-bonded silica 1 0 2 ± 5 . 2 7 9 ± 6 . 1 8 0 ± 8 . 8
Florisil 3 9 ± 1 . 4 8 0 ± 4 . 3 1 4 ± 0 . 3
Silica gel 7 ± 0 . 3 7 0 ± 1 . 6 1 7 ± 0 . 2
ENVI-Carb 7 4 ± 6 . 7 7 3 ± 1 . 4 8 0 ± 7 . 4
ENVI-Carb/LC-NH2 5 4 ± 3 . 4 4 1 ± 2 . 9 5 2 ± 2 . 7