Research Article
Synthesis, Characterisation, Crystal Structure, and Antimicrobial and Larvicidal Studies of [Cu(2,2′-bipy)2SO4]·3CH4N2O·2H2O
Table 1
Crystal data and structure refinement for the complex Cu(2,2′-bipy
SO
4]·3CH
4N
2O·2H
2O.
| Empirical formula | C23H32CuN10O9S | Formula weight | 688.19 | Temperature/K | 293(2) | Crystal system | Monoclinic | Space group | C2/c | /Å | 20.155(4) | /Å | 20.858(4) | /Å | 14.425(3) | /° | 90.00 | /° | 96.51(3) | /° | 90.00 | Volume/Å3 | 6025(2) | | 8 | mg/mm3 | 1.517 | /mm−1 | 0.861 | (000) | 2856.0 | Crystal size/mm3 | 0.23 0.19 0.15 | 2Θ range for data collection | 3.84 to 56.62° | Index ranges | −25 ≤ ≤ 19, −27 ≤ ≤ 27, and −19 ≤ ≤ 12 | Reflections collected | 21903 | Independent reflections | 6624 [(int) = 0.0310] | Data/restraints/parameters | 6624/0/461 | Goodness of fit on | 1.031 | Final indexes [ > 2()] | = 0.0360, = 0.0878 | Final indexes [all data] | = 0.0642, = 0.0990 | Largest diff. peak/hole/e Å−3 | 0.32/−0.34 |
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