| Structural data | (1) | (2) |
| Empirical formula | Na3CoP3O10·12H2O | Na3NiP3O10·12H2O | Formula weight (g/mol) | 597 | 596.8 | Temperature (K) | 120 | 120 | Wavelength Mo (Å) | 1.54184 | 1.54184 | Crystal system, space group | Monoclinic, P21/n | Monoclinic, P21/n | Unit cell dimensions | | | a (Å), α (°) | 15.0263(3), 90 | 14,9906(4), 90 | b (Å), β (°) | 9.1972(2), 90.0492(16) | 9,1628(2), 90.098(2) | c (Å), γ (°) | 14.6654(3), 90
| 14,6660(4), 90 | Volume (Å3), Z | 2026.76(7), 4 | 2014.46(9), 4 | (Mg/m3) | 1.9559 | 1.967 | Absorption coefficient (mm−1) | 10.499 | 5.267 | F(000) | 1220 | 1224 | Crystal size (mm) | 0.3416 * 0.1882 * 0.1274
| 0.5021 * 0.0801 * 0.0527 | Crystal shape, colour | Prism, pink | Needle, colorless | Limiting indices | | | Reflections collected | 3534 | 3181 | Independent reflections | 3456 | 3107 | Diffractometer | Oxford Diffraction Ltd. | Oxford Diffraction Ltd. | Data/restraints/parameters | 3534/24/336 | 3181/24/336 | Goodness-of-fit on | 1.61 | 2.11 | Final R indices | = 0.0261, = 0.0735 | = 0.0277, = 0.0904 | R indices (all data) | = 0.0267, = 0.0738 | = 0.0284, = 0.0907 |
|
|