Research Article

Superfast Set, Strong and Less Degradable Mineral Trioxide Aggregate Cement

Table 1

Materials used in this study, liquids used for mixing, cements’ codes and pH measurements.

Materials (code, manufacturer)Liquids for mixingCode after mixing with liquidImmediate pH30 min pH

Portland cement type I (PC, Quikrete® Number 1124, Atlanta, GA, USA)(a) Distilled water “W,” provided by manufacturers.
(b) Experimental liquid “H.” 0.3 g calcium chloride dihydrate (CaCl2⋅2H2O) + 0.075 g fumed silica (Aerosil EG 50, Evonik) + 0.3 g hydroxyapatite [Ca10(PO4)6(OH)2] + 1 ml distilled water.
(c) Experimental liquid “P,” similar to “H” except that the 0.3 g hydroxyapatite was replaced by 0.3 g calcium hydrogen phosphate.
Powder mixed with distilled waterPC-W
Powder mixed with liquid “H”PC-H
Powder mixed with liquid “P”PC-P

Grey ProRoot® MTA (GMTA, Dentsply, Tulsa Dental Specialties, UK)(a) Distilled water “W.” Provided by manufacturers.
(b) Experimental liquid “H,” 0.3 g calcium chloride dihydrate (CaCl2⋅2H2O) + 0.075 g fumed silica (Aerosil EG 50, Evonik) + 0.3 g hydroxyapatite [Ca10(PO4)6(OH)2] + 1 ml distilled water.
(c) Experimental liquid “P.” Similar to “H” except that the 0.3 g hydroxyapatite was replaced by 0.3 g calcium hydrogen phosphate.
Powder mixed with distilled waterGMTA-W
Powder mixed with liquid “H”GMTA-H
Powder mixed with liquid “P”GMTA-P

White ProRoot® MTA (WMTA, Dentsply, Tulsa Dental Specialties, UK)(a) Distilled water “W.” Provided by manufacturers.
(b) Experimental liquid “H.” 0.3 g calcium chloride dihydrate (CaCl2⋅2H2O) + 0.075 g fumed silica (Aerosil EG 50, Evonik) + 0.3 g hydroxyapatite [Ca10(PO4)6(OH)2] + 1 ml distilled water.
(c) Experimental liquid “P.” Similar to “H” except that the 0.3 g hydroxyapatite was replaced by 0.3 g calcium hydrogen phosphate.
Powder mixed with distilled waterWMTA-W
Powder mixed with liquid “H”WMTA-H
Powder mixed with liquid “P”WMTA-P