A High Throughput Method for Measuring Polycyclic Aromatic Hydrocarbons in Seafood Using QuEChERS Extraction and SBSE

Table 2

MSD SIM method conditions; quantifier in bold.

Group	RT^1 (min)	Ions monitored
1	2.5	(102, 50), (126, 50), (128, 50)
2	7.6	(115, 50), (141, 50), (142, 50)
3	9.0	(151, 20), (152, 20), (153, 20), (154, 20)
4	10.0	(165, 50), (166, 50), (167, 50)
5	11.5	(176, 50), (178, 50), (179, 50)
6	13.5	(200, 50), (202, 50), (203, 50)
7	15.5	(226, 50), (228, 50), (229, 50)
8	17.4	(126, 50), (252, 50), (253, 50)
9	19.2	(138, 20), (139, 20), (276, 20), (277, 20), (278, 20), (279, 20)

Group 1: naphthalene; Group 2: 2-methylnaphthalene; Group 3: acenaphthylene, acenaphthene; Group 4: fluorene; Group 5: phenanthrene, anthracene; Group 6: fluoranthene, pyrene; Group 7: benzoanthracene, chrysene; Group 8: benzofluoranthene, benzofluoranthene, Benzopyrene; Group 9: benzoperylene.
¹RT is the retention time for the start of the SIM group window.